fig6
Figure 6. Concentration-dependent kinetic analysis of Ni2Mo-NiOOH/MoOx and Ni2Mo/NF catalysts. (A and C) LSV curves of Ni2Mo-NiOOH/MoOx and Ni2Mo/NF at different urea concentrations (0.0125-0.33 M); (B and D) Linear fitting relationships between j1/2 and urea concentration for Ni2Mo-NiOOH/MoOx and Ni2Mo/NF, respectively, reflecting the concentration dependence toward urea oxidation; (E and G) LSV curves of Ni2Mo-NiOOH/MoOx and Ni2Mo/NF at different KOH concentrations (0.1-1 M); (F and H) Log(j)-Log[KOH] fitting curves for Ni2Mo-NiOOH/MoOx and Ni2Mo/NF, respectively, used to determine the apparent reaction order with respect to OH- concentration. RHE: Reversible hydrogen electrode; NF: nickel foam; KOH: potassium hydroxide; LSV: linear sweep voltammetry; j1/2: half-wave current density.



