fig5

Unveiling proton-regulated Mo=O/Mo-O<sup>-</sup> centers in reconstructed Ni<sub>2</sub>Mo-NiOOH/MoO<sub>x</sub> interfaces toward accelerated proton-coupled electron transfer for urea oxidation reaction

Figure 5. Effects of different concentrations of MoO42- and Ni2+ in the electrolyte on the UOR electrocatalytic performance of various catalytic electrodes. (A-D) LSV curves of Ni2Mo-NiOOH/MoOx, Ni2Mo/NF, Ni-NiOOH and Ni/NF catalytic electrodes with 0-5 mM MoO42- added into the electrolyte containing 1 M KOH and 0.33 M CO(NH2)2; (E-H) LSV curves of the above catalytic electrodes with 0-50 μM Ni2+ added into the electrolyte. RHE: Reversible hydrogen electrode; KOH: potassium hydroxide; LSV: linear sweep voltammetry; UOR: urea oxidation reaction.

Catalysis, Energy and Environment
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